Published at : 16 Dec 2019
Volume : IJtech
Vol 10, No 8 (2019)
DOI : https://doi.org/10.14716/ijtech.v10i8.3476
Dharmanto | Department of Mechanical Engineering, Faculty of Engineering, Universitas Indonesia, Kampus UI Depok, Depok 16424, Indonesia |
Sugeng Supriadi | Department of Mechanical Engineering, Faculty of Engineering, Universitas Indonesia, Kampus UI Depok, Depok 16424, Indonesia |
Ario Sunar Baskoro | Department of Mechanical Engineering, Faculty of Engineering, Universitas Indonesia, Kampus UI Depok, Depok 16424, Indonesia |
The low-cost plasma atomizer in the present
study successfully synthesized stainless steel spherical powder using an energy
source of less than 3 kVA. Repeated testing was conducted to examine the
resulting spherical powder, among other observations, using a digital
microscope (Dino-Lite AM4115), scanning electron microscopy (SEM-FEI-Inspect
F50), and energy dispersive spectroscopy (EDS). To ensure the purity of the
resulting 316L stainless steel spherical powder, EDS was used for qualitative
and quantitative elemental analysis. The results showed that the 316L stainless
steel spherical powder particles varied in size from 26 µm to 180 µm with
average particle diameters of approximately 82.6 µm, making them ideal for
biomedical applications. The results of the feed metal flow rate on the powder
weight percentages for particle sizes <50 µm for 2 mm3/s feed
metal flow, 3 mm3/s feed metal flow, and 4 mm3/s feed
metal flow were 26.04%, 28.04%, and 13.09%, respectively. It is possible that
this could occur because greater metal flow rates require greater plasma energy
to form liquid metal droplets, so that a lower metal flow rate at the same
energy consumption makes it possible to produce more metal powder in smaller
particles.
Plasma atomizer; Powder technology; Spherical particle; Stainless steel powder
The
metal manufacturing industry is currently interested in developing metal powder
technology for production cost efficiency. One of the applications of metal
powder technology is as a feedstock for metal
injection molding (MIM) (Suharno et al., 2019; Supriadi et al.,
2019). MIM can produce lower surface roughness values ??compared
to investment casting (Suharno et al., 2018). MIM is advantageous mainly due to its
significant technological cost savings compared with the use of machinery (Schieleper, 2006; Supriadi et al.,
2015). Metal powder technology enables reductions in waste
material production. Metal powder technology can be classified as a green
technology because it can reduce more residual waste material than other
conventional fabrication technologies such as five-axis CNC machining (Higashitani et al., 2019). At this time, the atomization process is
a suitable choice for producing metal powder because atomization is capable of
producing large amounts of powder with high purity (Boulos, 2004). Atomization processes for making metal
powder include water atomization, gas atomization (Zhao et al., 2007), centrifugal atomization (Sungkhaphaitoon et al., 2013), plasma atomization, and plasma rotating
electrodes process atomization (Dawes et al., 2015).
The
atomization process that uses a plasma arc has a high heat source density that
can melt various
A plasma atomizer is capable of producing a powder with
particle diameters of 50 µm (Chen et
al., 2018). Powder with particles of this size can be applied as the
primary raw material for making medical devices (Grenier & Allaire, 1997; Baskoro & Supriadi, 2019). One of the characteristics of high-quality metal powder is the
perfect spherical shapes of the particles and a narrow size distribution, which
can improve the flowability of the powder.
The current challenge of
using plasma atomization is its high cost, partly because the process requires
a large energy source. The energy sources used generally have a power of
approximately 20 kVA-600 kVA (Tsantrizos et al., 1998; Dignard & Boulos, 2000; Boulos, 2004; Dawes et al., 2015). In the present study, a
plasma atomizer with low-cost equipment was designed and built as a solution to
the high cost of plasma atomization. A plasma atomizer was fabricated with a
power of 3 kVA without the need to use a melt bath, so the plasma atomization
process is faster than the gas atomization or water atomization processes. The
plasma atomization process has been made to produce stainless steel spherical
powder particles with a diameter of less than 50 µm.
The results of the experiments in this study show that the plasma atomizer successfully synthesized the spherical metal powder using an energy source of less than 3 kVA. The plasma atomizer can produce perfectly spherical stainless steel powder particles. The sizes of the resulting 316L stainless steel spherical powder particles vary from 26 µm to 180 µm. The average particle diameter is approximately 82.6 µm. The results of the flow rate on the powder weight percentages at particle sizes <50 µm for 2 mm3/s feed metal flow, 3 mm3/s feed metal flow, and 4 mm3/s feed metal flow are 26.04%, 28.04%, and 13.09%, respectively. It is possible that this could occur because greater metal flow rates require greater plasma energy to form liquid metal droplets, so that a lower metal flow rate makes it possible to produce more metal powder in smaller particles. The resulting 316L stainless steel spherical powder is likely to be used in biomedical manufacturing applications. Based on the above research, fascinating research could be conducted to find the optimal parameters in the plasma atomization in order to produce particle sizes that are suitable for biomedical equipment manufacturing applications.
This research was
supported by the Ministry of Research and Technology of the Republic of
Indonesia through the Excellent Applied Research in Higher Education scheme
(contract number: NKB-1744/ UN2.R3.1/ HKP.05.00/ 2019).
Baskoro, A.S., Masuda
R., Suga Y., 2011. Comparison of Particle Swarm Optimization and Genetic
Algorithm for Molten Pool Detection in Fixed Aluminum Pipe Welding. International Journal of Technology,
Volume 2(1), pp. 74–83
Baskoro, A.S., Supriadi
S., 2019. Review on Plasma Atomizer Technology for Metal Powder. In: Proceedings of the MATEC Web of
Conferences, 2019: EDP Sciences, 05004
Baskoro A.S., Tandian
R., Edyanto A., Saragih A.S., 2019. Automatic Tungsten Inert Gas (TIG) Welding
using Machine Vision and Neural Network on Material SS304. In: Proceedings of the 2016 International
Conference on Advanced Computer Science and Information Systems (ICACSIS), 2016:
IEEE, pp. 427–32
Becker, B., D Bolton J.,
1997. Corrosion Behaviour and Mechanical Properties of Functionally Gradient
Materials Developed for Possible Hard-tissue Applications. Journal of Materials Science: Materials in Medicine, Volume 8(12),
pp. 793–797
Boulos, M., 2004. Plasma Power Can Make Better Powders. Metal
Powder Report 59, pp. 16–21
Brooks, A. J., Ge J.,
Kirka M. M., Dehoff R. R., Bilheux H. Z., Kardjilov N., Manke I., Butler, L.G., 2017. Porosity Detection
in Electron Beam-melted Ti-6Al-4V using High-resolution Neutron Imaging and
Grating-based Interferometry. Progress in
Additive Manufacturing, Volume 2(3), pp. 125–132
Chen, G., Zhao, S., Tan,
P., Wang, J., Xiang, C., Tang, H., 2018. A Comparative Study of Ti-6Al-4V Powders
for Additive Manufacturing by Gas Atomization, Plasma Rotating Electrode
Process and Plasma Atomization. Powder
Technology, Volume 333, pp. 38–46
Chu, P.K., Chen, J.,
Wang, L., Huang, N., 2002. Plasma-surface
Modification of Biomaterials. Materials Science and Engineering: R: Reports
36, pp. 143–206
Cunningham, R., Narra,
S.P., Montgomery, C., Beuth, J., Rollett, A., 2017a. Synchrotron-based X-ray Microtomography
Characterization of the Effect of Processing Variables on Porosity Formation in
Laser Power-bed Additive Manufacturing of Ti-6Al-4V. JOM, Volume 69(3), pp. 479–484
Cunningham, R., Nicolas,
A., Madsen, J., Fodran, E., Anagnostou, E., Sangid, M.D., Rollett, A.D., 2017b.
Analyzing the Effects of Powder and Post-processing on Porosity and Properties
of Electron Beam Melted Ti-6Al-4V. Materials Research Letters, Volume 5(7), pp. 516–525
Dawes, J., Bowerman,
R., Trepleton, R., 2015. Introduction to the Additive Manufacturing Powder
Metallurgy Supply Chain. Johnson Matthey
Technology Review, Volume 59(3), pp. 243–256
Dewidar, M., 2012.
Influence of Processing Parameters and Sintering Atmosphere on the Mechanical
Properties and Microstructure of Porous 316L Stainless Steel for Possible Hard-tissue
Applications. International Journal of Mechanical &
Mechatronics Engineering, Volume 12, pp. 10–24
Dignard, N., Boulos, M.,
2000. Powder Spheroidization using Induction Plasma Technology. In: Proceedings of the ITSC 2000: 1st
International Thermal Spray Conference, 2000, pp. 887–893
Dion, D.A.C.,
Francois, P., 2019. Method for
Cost-Effective Production of Ultrafine Spherical Powders at Large Scale using
Thruster-assisted Plasma Atomization. Google Patents
Grenier, S.,
Allaire, F., 1997. Plasma Atomization
Gives Unique Spherical Powders. Metal Powder Report 52, pp. 34–37
Heaney, D., 2012. Designing for Metal Injection Molding (MIM).
Handbook of Metal Injection Molding.
Elsevier, pp. 29–49
Higashitani, K., Makino,
H., Matsusaka, S., 2019. Powder Technology
Handbook. CRC Press.
Hutmacher, D.W., 2000. Scaffolds in Tissue Engineering Bone And Cartilage.
The Biomaterials: Silver Jubilee Compendium. Elsevier, 175–189
Ismail, M.I.S., Taha,
Z., 2014. Surface Hardening of Tool Steel by Plasma Arc with Multiple Passes. International Journal of Technology,
Volume 5(1), pp. 79–87
Knight, R., Smith, R.,
Apelian, D., 1991. Application of Plasma Arc Melting Technology to Processing
of Reactive Metals. International
Materials Reviews, Volume 36(1),
pp. 221–252
Liu, S.X., Liu, J.L.,
Li, X.S., Zhu, X., Zhu, A.M., 2015. Gliding Arc Plasma Synthesis of Visible-Light Active C?doped Titania
Photocatalysts. Plasma Processes and
Polymers, Volume 12(5), pp. 422–430
Lü, Y.-H., Liu, Y.-X.,
Xu, F.-J., Xu, B.-S., 2013. Plasma Transferred Arc Forming Technology for Remanufacture.
Advances in Manufacturing, Volume 1(2), pp. 187–190
Luo, W., 2003. The Corrosion
Resistance of 0Cr19Ni9 Stainless Steel Arc Welding Joints with and Without Arc
Surface Melting. Materials Science and
Engineering: A, Volume 345(1–2), pp. 1–7
Saryanto, H., Sebayang,
D., 2017. The Simple Fabrication of Nanorods Mass Production for the Dye-sensitized
Solar Cell. In: Proceedings of the
MATEC Web of Conferences, 2017: EDP Sciences, 03006
Schieleper, G., 2006. A Manufacturing Process for Precision
Engineering Components. Powder Metallurgy Association, United Kingdom
Suharno, B., Mawardi,
F., Dewantoro, S., Irawan, B., Doloksaribu, M., Supriadi, S., 2019. Effect of Powder
Loading on Local Feedstock Injection Behavior for Fabrication Process of Orthodontic
Bracket SS 17-4 PH using Metal Injection Molding. In: Proceedings of the AIP Conference Proceedings, 2019: AIP
Publishing, 020030
Suharno, B., Suharno, L.P., Saputro, H.R., Irawan, B., Prasetyadi, T., Ferdian, D., Supriyadi, S., 2018. Surface Quality and Microstructure of Low-vacuum Sintered Orthodontic Bracket 17-4 PH Stainless Steel Fabricated by MIM Process. In: Proceedings of the AIP Conference Proceedings, 2018: AIP Publishing, 020030
Sungkhaphaitoon, P.,
Likhidkan W., Kitjaidiaw S., Wisutmethangoon S., Plookphol T., 2013. Effect of
Atomizer Disc Geometry on Zinc Metal Powder Production by Centrifugal
Atomization. In: Proceedings of the
Applied Mechanics and Materials, Volume 271–272, pp. 232–236
Supriadi, S., Dewantoro,
S., Mawardi, F. A., Irawan, B., Doloksaribu, M., Suharno, B., 2019. Preparation
of Feedstock using Beeswax Binder and SS 17-4PH Powder for Fabrication Process of
Orthodontic Bracket by Metal Injection Molding. In: Proceedings of the AIP Conference Proceedings, 2019: AIP
Publishing, 020029
Supriadi S., Sitanggang
T.W., Irawan B., Suharno B., Kiswanto G., Prasetyadi T., 2015. Orthodontic Bracket
Fabrication using the Investment Casting Process. International Journal of Technology, Volume 6(4), pp.
613–621
Tammas-Williams, S.,
Withers, P., Todd, I., Prangnell, P., 2016. Porosity Regrowth during Heat
Treatment of Hot Isostatically Pressed Additively Manufactured Titanium
Components. Scripta Materialia,
Volume 122, pp. 72–76
Tsantrizos, P.G.,
Allaire, F., Entezarian, M., 1998. Method
of Production of Metal and Ceramic Powders by Plasma Atomization. Google
Patents
Wang, J., Kusumoto, K.,
Nezu, K. 2000. Plasma Arc Cutting Torch Tracking Control. In: Proceedings of the 6th International Workshop on
Advanced Motion Control. Proceedings (Cat. No. 00TH8494), 2000: IEEE, 345–350